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Stiffness and hardness gradients obtained by laser surface treatment of aged beta-Ti alloys: The role of omega phase

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dc.contributor.author da Costa, Fernando Henrique es_ES
dc.contributor.author Sallica-Leva, Edwin es_ES
dc.contributor.author Mello, Mariana Gerardi es_ES
dc.contributor.author Amigó, Vicente es_ES
dc.contributor.author Caram, Rubens es_ES
dc.contributor.author Fogagnolo, Joao Batista es_ES
dc.date.accessioned 2024-11-20T19:10:05Z
dc.date.available 2024-11-20T19:10:05Z
dc.date.issued 2023-08-25 es_ES
dc.identifier.issn 0257-8972 es_ES
dc.identifier.uri http://hdl.handle.net/10251/212066
dc.description.abstract [EN] Functional gradient materials are interesting for optimizing the properties of engineering parts. Laser surface treatment makes it possible to obtain a stiffness gradient on titanium parts; such graded material is attractive due to the potential for orthopedic implant performance improvement and other applications as well. This work used laser surface treatment without fusion on two aged titanium alloys: Ti¿8Mo and Ti¿30Nb¿1Fe. This processing route aimed to fully dissolve the ¿-phase precipitates in a surface layer and, consequently, reduce the elastic modulus, producing a stiffness gradient from the surface to the inner material. Firstly, single tracks were obtained for different laser powers, kept constant the other parameters, aiming to determine the optimum condition to avoid surface fusion and produce the thickest-possible modified layer. Then, multi-track overlapping produced a modified continuous layer. The aged titanium alloys were characterized by optical and scanning electron microscopy and X-ray diffraction. The single tracks were characterized by stereoscopic and optical microscopy. Transmission electron microscopy and instrumented indentation completed the characterization of the laser-modified layer. Laser surface treatment produced a less-rigid surface layer in the Ti¿8Mo alloy due to the obtainment of ß and ¿¿¿ titanium phases with lower elastic modulus. The surface treatment did not change the material¿s hardness in this case. On the other hand, the precipitation of the ¿ phase during surface cooling of the Ti-30Nb-1Fe alloy prevented the elastic modulus from decreasing and increased the modified-layer hardness. Hence, the absence of ¿ phase precipitation is a condition to obtain a less-rigid surface layer by laser surface treatment on aged titanium alloys. es_ES
dc.description.sponsorship This study was financed by the Sao Paulo State Research Foundation (FAPESP, Brazil) (Process 2018/18293-8) and by the Coordination of Higher Education Personnel Improvement (CAPES, Brazil) - Finance Code 001. E. Sallica-Leva gratefully acknowledges the National Council for Scientific and Technological Development (CNPq, Brazil) for granting postdoctoral research fellowships (Grant no. 302115/2021-8). es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof Surface and Coatings Technology es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Titanium alloys es_ES
dc.subject Laser surface treatment es_ES
dc.subject Mechanical properties es_ES
dc.subject Stiffness-graded materials es_ES
dc.subject.classification CIENCIA DE LOS MATERIALES E INGENIERIA METALURGICA es_ES
dc.title Stiffness and hardness gradients obtained by laser surface treatment of aged beta-Ti alloys: The role of omega phase es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.surfcoat.2023.129697 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CNPq//302115%2F2021-8/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/FAPESP//2018%2F18293-8/ es_ES
dc.rights.accessRights Embargado es_ES
dc.date.embargoEndDate 2025-06-30 es_ES
dc.contributor.affiliation Universitat Politècnica de València. Escuela Técnica Superior de Ingenieros Industriales - Escola Tècnica Superior d'Enginyers Industrials es_ES
dc.description.bibliographicCitation Da Costa, FH.; Sallica-Leva, E.; Mello, MG.; Amigó, V.; Caram, R.; Fogagnolo, JB. (2023). Stiffness and hardness gradients obtained by laser surface treatment of aged beta-Ti alloys: The role of omega phase. Surface and Coatings Technology. 467. https://doi.org/10.1016/j.surfcoat.2023.129697 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.surfcoat.2023.129697 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 467 es_ES
dc.relation.pasarela S\495025 es_ES
dc.contributor.funder Fundação de Amparo à Pesquisa do Estado de São Paulo es_ES
dc.contributor.funder Coordenaçao de Aperfeiçoamento de Pessoal de Nível Superior, Brasil es_ES
dc.contributor.funder Conselho Nacional de Desenvolvimento Científico e Tecnológico, Brasil es_ES


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